Phthalic acid, bis-butyl ester
Formula：C16H22O4
Mol. Welght：278.34
CAS No.：84-74-2
Storage Temperature：20℃±4℃
Storageandhandling:
The RM should be stored in the original sealed bottle at the temperature given above.After use the bottle should be tightly closed and protected from moisture .
Purity：99.48% (g/g)
Expanded Uncertainty U= 0.30% (g/g)
The uncertainty of this standard is calculated in accordance with the lSO Guide 34 and EURACHEM/CITAC Guide - Quantifying Uncertainty in Analytical Measurement, Second Edition.The expanded uncertainty is U(exp)=u(RM)x k, where k is the coverage factor at the 95% confidence level (k=2). Uncertainty u(RM)is based on the combination of the uncertainties associated with each indvidual operation involved in the analysis of the product u(RM)=vu(char)2+u(bb)2+u(lts)2+u(sts)2; u(char) is the uncertainty of charactersation; u(bb) uncertainty of homogeneity test;u(lts) uncertaintyof stability test long-term; u(sts) uncertainty of stablitytest short-term.u(lts) and u(sts) are not incuded in the calculation as the stablity statement is based on real evidence opposed to simulation.
Minimum sample: 1 mg is recommended as the minimal sample amount.If less material is used it is recommended to increase the ceritfied uncertainty by a factor of two for half sample and a factor of four for a quarter of sample.
Intended use: Use this RM as calibrant for chromatography or any other analytical technique.
Analytical Data
Traceabity of dhromatography： To the intemational System of Units (SI).
Instrumert：GC/FID
Detectionc：FID
Column：Optima-5MS,0.25 um, 0.25 mm
lnj.-VolL：1μl
Flow：1.0 mL/min
Ret.Time：17.36min
lnjector：280°C
Initial Temp：60ºCfor 5 min
End Temp：280°C for 1min
Gradient：15°C/min
Comment
Traceabity： The balances used are calibrated with weights traceable to the national standards (DKD）.
Calibnated dass A glassware is used for volumetric measurements.
Water Content：<0.10% (g/g) by Karl-Fischer-Titration (U(exp) = 0.04% (g/g)).
Purity was determined by chromatographic assay, corrected by water content and/or residue solvents.
ldentity：EA, NMR RT, IR, MS
Attachment: Exemplary chromatogram of given method.
注：以上信息仅供参考，以产品附带证书为准。
