Certificate of Analysis
ISO Guide 34 Reference Material
Product identification
Articie Code:DRE-C12730000 Lot Number: G146122
Article Name: 2,3-Dimethylphenol Expiry Date: 1108.2023
Formula: C8H100 Storage Temperature: 20°℃±4℃
Mol. Weight: 122.17
CAS NO.: 526-75-0
Storage and handling: The RM should be stored in the original sealed bottle at the temperatur given above.After use the bottle should be tightly cosed and protected from moisture and light.The expiny date is valid for original sealed botties under recommended storage conditions only.
Purity: 98.92%(/g)
Expanded Uncertainty U= 0.30%(/g)
The uncertainty of this standard is calcuiated in accordance with the lS0 Guide 34andURACHEM/CITAC Guide-Quantifying Uncertainty in Analytical Measurement, Second Edition. The expanded uncertainty isU(exp)=u(RMxk wherek is the coverage factor at the 95% confidence leve(k=2).Uncertaintyu(RM) is based on the combination of the uncertainties associated with each individual peration involved in the analysis of the product:u(RM)=vu(char)2+u(bb+u(lts)2+u(sts)’;ufchar) is the uncertainty of purity determination;u(bb)uncertainty of homogeneity test; ufits) uncertainty of stability test long-term;u(sts)uncertainty of stabillty test short-term.ulits)andu(sts)are not included in the calculation as the stability statement is based on real evidence opposed to simulation.
Minimum sample:1 mg is recommended as the minimal sample amount.Iif less material is used,it is recommended to increase the certified uncertainty by a factor of two for half sample and a factor of four for a quarter of sample
Intended use: Use this RM as calibrant for chromatography or any other analytical technique.
Analytical Data
Traceability of chromatography: To the intenational System of Units (SI)
Instrument: HPLC/DAD Method Details
Detection: DAD Acetonitrile:Water+0.5% H3PO4 4:1
Column: ReproSil 100C18 5um250x3mm
Inj.-Vol.: 3 μl
Flow: 1.0ml/min
Ret.Time: 1.60 min
Comment
Traceability: The balances used are calibrated with weights traceable to the national standards(DKD)
Calibrated class A glassware is used for volumetric measurements.
Certificate Revision1
Water Content:0.10%(g/g)by Karl-Fischer-Titration(U(exp)=0.03%(g/g))
identity: EA,NMR,RT,IR,UV,MS
Data file: 12730000-11.dx Instrument: DAD4
Sample name: 70802AL G146122 Sequence Name: 04082017-3
Inj. volume [ul]: 3.0 Injection date: 8/4/2017 7:19:45PM
Acq. method: 41PK.amx Location: 10
Sample Description 2,3-Dimethylphenol
注:以上信息仅供参考,以产品附带证书为准。